To synthesize virtual powder patterns from spot-finding results, highly accurate spot positions are required; therefore, the experimental geometry must be measured with high accuracy as well. We achieved this in a two-step process: first, the beam centre and detector distance were determined using powder diffraction … See more Benzeneselenol (97%, 375152), diphenyl ditelluride (98%, 384127), silver (I) oxide (99%, 221163), silver powder (>99.9%, 327077), and thiophenol (97%, T32808) were used as received from Sigma Aldrich. Microcrystalline silver … See more Thiorene and tethrene were transported as dry solids to the Coherent X-ray Imaging endstation at the Linac Coherent Light Source12 for smSFX experiments. Solvated samples were delivered to the XFEL interaction point … See more Having prepared of the order of 1018 crystals, we used a Rayleigh jet injector system40 at a high flow rate of ~150 µl min−1 to reduce the possibility of clogging the capillary lines. The jet was positioned to intersect the 1 µm … See more We use the following approach to construct the powder pattern for unit-cell determination: (1) The DIALS spot-finder is used to harvest Bragg … See more WebA good approach to determine the spacegroup is to initially scale the data in the lowest symmetry spacegroup for the crystal class and then select use the Check Space Group …
(PDF) Scaling and assessment of X-ray data quality
WebJun 6, 2005 · A requirement for the scaling and merging of intensities is knowledge of the Laue group and point-group symmetries: the possible symmetry of the diffraction pattern … WebJun 2, 2024 · Scaling Merging Serial femtosecond crystallography Download protocol PDF Springer Nature is developing a new tool to find and evaluate Protocols. Learn more 1 Introduction: The Unique Features of Crystallographic Data from an XFEL cropsey\u0027s creepy con
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WebDec 2, 2013 · In order to generate high power laser radiation it is often necessary to combine multiple lasers into a single beam. The recent advances in high power spectral beam … WebThe scaling procedure in iMosflm is not meant for careful scaling and merging; instead, it's supposed to give you a decent idea about the quality of your integration, estimate the correct space group and resolution limits, and inform the next indexing, lattice refinement, or integration approach if necessary. In cases of really nice data ... WebA multi-dimensional scaling procedure is first used to identify data sets with large non-isomorphism relative to clusters of other data sets. Within each cluster that it identifies, … cropsey \\u0026 cropsey